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Tipo de Documento: Artigo
Título : 1-(5-Bromo-2-oxoindolin-3-ylidene)-4- phenylthiosemicarbazide
Autor : Bandeira, Katlen Crhistian Tribuzy
Bresolin, Leandro
Näther, Christian
Jess, Inke
Oliveira, Adriano Bof de
Fecha de publicación : 2013
Resumen: In the title compound, C15H11BrN4OS, the least-squares plane through the 5-bromoisatin fragment forms a dihedral angle of 13.63 (14) with the phenyl ring. The molecular conformation features intramolecular N—HN and N—HO hydrogen bonds. In the crystal, molecules are connected via pairs of N— HO interactions into centrosymmetric dimers. Additionally, – stacking interactions link molecules into chains parallel to the a axis with short CC distances being observed between the phenyl and thiocarbonyl [3.236 (8) A˚ ] groups and between the thiocarbonyl and carbonyl [3.351 (4) A˚ ] groups of stacked molecules.
Palabras clave : Single-crystal X-ray study
T = 200 K
Mean (C–C) = 0.005 A˚
R factor = 0.046
WR factor = 0.105
Data-to-parameter ratio = 14.6
ISSN : 1600-5368
Es parte de: Acta Crystallographica Section E
Idioma : eng
Institución / Editorial : International Union of Crystallography
Citación : BANDEIRA, K. C. T. et al. 1-(5-Bromo-2-oxoindolin-3-ylidene)-4-phenylthiosemicarbazide. Acta crystallographica Section E, Chester, v. 69, n. 8, p. o1337-o1338, 2013. Disponível em: https://journals.iucr.org/e/issues/2013/08/00/fy2102/index.html. Acesso em: 21 out. 2025.
License: Creative Commons Atribuição 2.0 Reino unido: Inglaterra e País de Gales (CC BY 2.0 UK)
URI : https://ri.ufs.br/jspui/handle/riufs/23589
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