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https://ri.ufs.br/jspui/handle/riufs/23696| Document Type: | Artigo |
| Title: | 1-(2H-1,3-Benzodioxol-5-yl) ethanone thiosemicarbazone |
| Authors: | Oliveira, Adriano Bof de Farias, Renan Lira de Näther, Christian Jess, Inke Bresolin, Leandro |
| Issue Date: | 2013 |
| Resumo : | In the title compound, C10H11N3O2S, the 1,3-benzodioxole and hydrazinecarbothioamide fragments are nearly planar [(mean deviations from planarity for non-H atoms of 0.0325 (12) A˚ and 0.0707 (10) A˚ , respectively] and subtend a dihedral angle of 29.06 (5). In the crystal, molecules are linked by pairs of almost linear N—HS hydrogen bonds, forming inversion dimers. These dimers are additionally connected by weaker and strongly bent N—HS interactions into chains along [101]. There is one additional weak N— HO contact which, if considered as an interaction, leads to the formation of a three-dimensional network. |
| Keywords: | Single-crystal X-ray study T = 200 K Mean (C–C) = 0.002 A˚ R factor = 0.037 WR factor = 0.107 Data-to-parameter ratio = 15.7 |
| ISSN: | 1600-5368 |
| Is part of: | Acta Crystallographica Section E |
| Language: | eng |
| Publisher / Institution : | International Union of Crystallography |
| Citation: | OLIVEIRA, A. B. et al. 1-(2H-1,3-Benzodioxol-5-yl) ethanone thiosemicarbazone. Acta crystallographica Section E, Chester, v. 69, n. 5, p. o644, 2013. Disponível em: https://journals.iucr.org/e/issues/2013/05/00/qk2055/index.html. Acesso em: 3 nov. 2025. |
| License: | Creative Commons Atribuição 2.0 Reino unido: Inglaterra e País de Gales (CC BY 2.0 UK) |
| URI: | https://ri.ufs.br/jspui/handle/riufs/23696 |
| Appears in Collections: | DQI - Artigos de periódicos |
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| File | Description | Size | Format | |
|---|---|---|---|---|
| 1-(2H-1,3-Benzodioxol-5-yl)EthanoneThiosemicarbone.pdf | 416,6 kB | Adobe PDF |  View/Open |
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