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https://ri.ufs.br/jspui/handle/riufs/24730| Document Type: | Artigo |
| Title: | Crystal structure of 4-hydroxy-3-methoxybenzaldehyde 4-methylthiosemicarbazone methanol monosolvate |
| Authors: | Oliveira, Adriano Bof de Beck, Johannes Landvogt, Christian Feitosa, Bárbara Regina Santos |
| Issue Date: | 2015 |
| Resumo : | In the title solvate, C15H15N3O2SCH3OH, the thiosemicarbazone molecule is approximately planar; the maximum deviation from the mean plane is 0.4659 (14) A˚ and the dihedral angle between the aromatic rings is 9.83 (8). This conformation is supported by an intramolecular N— HN hydrogen bond. In the crystal, the thiosemicarbazone molecules are linked into dimers by pairs of N—HS hydrogen bonds, thereby generating R2 2 (8) loops. The methanol solvent molecule bonds to the thiosemicarbazone molecule through a bifurcated O—H(O,O) hydrogen bond and also accepts an O—HO link from the thiosemicarbazone molecule. Together, these links generate a three-dimensional network. |
| Keywords: | Crystal structure Bifurcated hydrogen bond Thiosemicarbazone derivative from natural product Vanillin |
| ISSN: | 2056-9890 |
| Is part of: | Acta Crystallographica Section E |
| Language: | eng |
| Publisher / Institution : | International Union of Crystallography |
| Citation: | OLIVEIRA, A. B. et al. Crystal structure of 4-hydroxy-3-methoxybenzaldehyde 4-methylthiosemicarbazone methanol monosolvate. Acta Crystallographica Section E, Chester, v. 71, n. 5, 2015. Disponível em: https://journals.iucr.org/e/issues/2015/05/00/hb7402/index.html. Acesso em: 10 mar. 2026. |
| License: | Creative Commons Atribuição 2.0 Reino unido: Inglaterra e País de Gales (CC BY 2.0 UK) |
| Identifier: | https://doi.org/10.1107/S2056989015007227 |
| URI: | https://ri.ufs.br/jspui/handle/riufs/24730 |
| Appears in Collections: | DQI - Artigos de periódicos |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| CrystalStructure4-hydroxy-3-methoxybenzaldehyde.pdf | 354,04 kB | Adobe PDF |  View/Open |
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