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Tipo de Documento:	Artigo
Título:	Crystal structure of (E)-2-[1-(benzo[d]- [1,3]dioxol-5-yl) ethylidene]-N-methylhydrazine-1-carbothioamide
Autor(es):	Oliveira, Adriano Bof de Näther, Christian Jess, Inke Farias, Renan Lira de Ribeiro, Iasmin Alves
Data do documento:	2015
Resumo:	In the title compound, C11H13N3O2S, there is a short intramolecular N—HN contact. The benzo[d][1,3]dioxole ring system is approximately planar (r.m.s. deviation = 0.025 A˚ ) and makes a dihedral angle of 56.83 (6) with the mean plane of the methylthiosemicarbazone fragment [–N— N—C( S)—N—C; maximum deviation = 0.1111 (14) A˚ for the imino N atom]. In the crystal, molecules are linked via pairs of N—HS hydrogen bonds, forming inversion dimers. The dimers are connected by N—HS hydrogen bonds into layers parallel to (100). The H atoms of both methyl groups are disordered over two sets of sites and were refined with occupancy ratios of 0.5:0.5 and 0.75:0.25.
Palavras-chave:	Crystal structure Thiosemiarbazone 30,40-(methylenedioxy) acetophenone 4-methylthiosemicarbazone Hydrogen bonding Twodimensional network
ISSN:	2056-9890
Parte de :	Acta Crystallographica Section E
Idioma:	eng
Instituição/Editora:	International Union of Crystallography
Citação:	OLIVEIRA, A. B. et al. Crystal structure of (E)-2-[1-(benzo[d]- [1,3]dioxol-5-yl) ethylidene]-N-methylhydrazine-1-carbothioamide. Acta Crystallographica Section E, Chester, v. 71, n. 1, 2015. Disponível em: https://journals.iucr.org/e/issues/2015/01/00/su5032/index.html. Acesso em: 11 mar. 2026.
Licença:	Creative Commons Atribuição 2.0 Reino unido: Inglaterra e País de Gales (CC BY 2.0 UK)
Identificador:	https://doi.org/10.1107/S2056989014026395
URI:	https://ri.ufs.br/jspui/handle/riufs/24733
Aparece nas coleções:	DQI - Artigos de periódicos

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