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https://ri.ufs.br/jspui/handle/riufs/21376| Document Type: | Artigo |
| Title: | MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey |
| Authors: | Bezerra, Débora Santos Silva Silva, Marcell Mendes Santos Carvalho, Pedro Henrique Viana de Aquino, Adriano Navickiene, Sandro |
| Issue Date: | 2010 |
| Resumo : | A method based on matrix solid-phase dispersion and gas chromatography-mass spectrometry to determine procymidone, malathion, bifenthrin and pirimicarb in honey is described. The best results were obtained using 1.0 g of honey, 1.0 g of silica-gel as dispersant sorbent and acetonitrile as eluting solvent. The method was validated by fortified honey samples at three concentration levels (0.2, 0.5 to 1.0 mg kg1 ). Average recoveries (n=7) ranged from 54 to 84%, with relative standard deviations between 3.7 and 8.5%. Detection and quantification limits attained by the developed method ranged from 0.02 to 0.08 mg kg-1 and 0.07 to 0.25 mg kg-1 for the honey, respectively. |
| Keywords: | Honey Pesticides Matrix solid-phase dispersion |
| ISSN: | 0100-4042 1678-7064 |
| Is part of: | Química Nova |
| Language: | eng |
| Publisher / Institution : | Sociedade Brasileira de Química |
| Citation: | BEZERRA, D. S. S. et al. MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey. Química Nova, São Paulo, v. 33, n. 6, p. 1348-1351, 2010. Disponível em: https://www.scielo.br/j/qn/a/bmL96zPk53vWDM9gb3hgTMr/?format=pdf&lang=en. Acesso em: 14 mar. 2025. |
| License: | Creative Commons Atribuição-NãoComercial 4.0 Internacional (CC BY-NC 4.0) |
| URI: | https://ri.ufs.br/jspui/handle/riufs/21376 |
| Appears in Collections: | DQI - Artigos de periódicos |
Files in This Item:
| File | Description | Size | Format | |
|---|---|---|---|---|
| MSPDProcedureHoney.pdf | 272,88 kB | Adobe PDF |  View/Open |
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