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Tipo de Documento:	Artigo
Título :	MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey
Autor :	Bezerra, Débora Santos Silva Silva, Marcell Mendes Santos Carvalho, Pedro Henrique Viana de Aquino, Adriano Navickiene, Sandro
Fecha de publicación :	2010
Resumen:	A method based on matrix solid-phase dispersion and gas chromatography-mass spectrometry to determine procymidone, malathion, bifenthrin and pirimicarb in honey is described. The best results were obtained using 1.0 g of honey, 1.0 g of silica-gel as dispersant sorbent and acetonitrile as eluting solvent. The method was validated by fortified honey samples at three concentration levels (0.2, 0.5 to 1.0 mg kg1 ). Average recoveries (n=7) ranged from 54 to 84%, with relative standard deviations between 3.7 and 8.5%. Detection and quantification limits attained by the developed method ranged from 0.02 to 0.08 mg kg-1 and 0.07 to 0.25 mg kg-1 for the honey, respectively.
Palabras clave :	Honey Pesticides Matrix solid-phase dispersion
ISSN :	0100-4042 1678-7064
Es parte de:	Química Nova
Idioma :	eng
Institución / Editorial :	Sociedade Brasileira de Química
Citación :	BEZERRA, D. S. S. et al. MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey. Química Nova, São Paulo, v. 33, n. 6, p. 1348-1351, 2010. Disponível em: https://www.scielo.br/j/qn/a/bmL96zPk53vWDM9gb3hgTMr/?format=pdf&lang=en. Acesso em: 14 mar. 2025.
License:	Creative Commons Atribuição-NãoComercial 4.0 Internacional (CC BY-NC 4.0)
URI :	https://ri.ufs.br/jspui/handle/riufs/21376
Aparece en las colecciones:	DQI - Artigos de periódicos

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