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Campo DC | Valor | Idioma |
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dc.contributor.author | Bezerra, Débora Santos Silva | - |
dc.contributor.author | Silva, Marcell Mendes Santos | - |
dc.contributor.author | Carvalho, Pedro Henrique Viana de | - |
dc.contributor.author | Aquino, Adriano | - |
dc.contributor.author | Navickiene, Sandro | - |
dc.date.accessioned | 2025-03-14T14:50:29Z | - |
dc.date.available | 2025-03-14T14:50:29Z | - |
dc.date.issued | 2010 | - |
dc.identifier.citation | BEZERRA, D. S. S. et al. MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey. Química Nova, São Paulo, v. 33, n. 6, p. 1348-1351, 2010. Disponível em: https://www.scielo.br/j/qn/a/bmL96zPk53vWDM9gb3hgTMr/?format=pdf&lang=en. Acesso em: 14 mar. 2025. | pt_BR |
dc.identifier.issn | 0100-4042 | - |
dc.identifier.issn | 1678-7064 | - |
dc.identifier.uri | https://ri.ufs.br/jspui/handle/riufs/21376 | - |
dc.language | eng | pt_BR |
dc.publisher | Sociedade Brasileira de Química | pt_BR |
dc.relation.ispartof | Química Nova | pt_BR |
dc.subject | Honey | eng |
dc.subject | Pesticides | eng |
dc.subject | Matrix solid-phase dispersion | eng |
dc.title | MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey | pt_BR |
dc.type | Artigo | pt_BR |
dc.identifier.license | Creative Commons Atribuição-NãoComercial 4.0 Internacional (CC BY-NC 4.0) | pt_BR |
dc.description.resumo | A method based on matrix solid-phase dispersion and gas chromatography-mass spectrometry to determine procymidone, malathion, bifenthrin and pirimicarb in honey is described. The best results were obtained using 1.0 g of honey, 1.0 g of silica-gel as dispersant sorbent and acetonitrile as eluting solvent. The method was validated by fortified honey samples at three concentration levels (0.2, 0.5 to 1.0 mg kg1 ). Average recoveries (n=7) ranged from 54 to 84%, with relative standard deviations between 3.7 and 8.5%. Detection and quantification limits attained by the developed method ranged from 0.02 to 0.08 mg kg-1 and 0.07 to 0.25 mg kg-1 for the honey, respectively. | pt_BR |
dc.description.local | São Paulo, SP | pt_BR |
Aparece nas coleções: | DQI - Artigos de periódicos |
Arquivos associados a este item:
Arquivo | Descrição | Tamanho | Formato | |
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MSPDProcedureHoney.pdf | 272,88 kB | Adobe PDF | ![]() Visualizar/Abrir |
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