1. Repositório Institucional da Universidade Federal de Sergipe - RI/UFS
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  3. DQI - Departamento de Química (São Cristóvão)
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Please use this identifier to cite or link to this item: https://ri.ufs.br/jspui/handle/riufs/21376
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dc.contributor.authorBezerra, Débora Santos Silva-
dc.contributor.authorSilva, Marcell Mendes Santos-
dc.contributor.authorCarvalho, Pedro Henrique Viana de-
dc.contributor.authorAquino, Adriano-
dc.contributor.authorNavickiene, Sandro-
dc.date.accessioned2025-03-14T14:50:29Z-
dc.date.available2025-03-14T14:50:29Z-
dc.date.issued2010-
dc.identifier.citationBEZERRA, D. S. S. et al. MSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honey. Química Nova, São Paulo, v. 33, n. 6, p. 1348-1351, 2010. Disponível em: https://www.scielo.br/j/qn/a/bmL96zPk53vWDM9gb3hgTMr/?format=pdf&lang=en. Acesso em: 14 mar. 2025.pt_BR
dc.identifier.issn0100-4042-
dc.identifier.issn1678-7064-
dc.identifier.urihttps://ri.ufs.br/jspui/handle/riufs/21376-
dc.languageengpt_BR
dc.publisherSociedade Brasileira de Químicapt_BR
dc.relation.ispartofQuímica Novapt_BR
dc.subjectHoneyeng
dc.subjectPesticideseng
dc.subjectMatrix solid-phase dispersioneng
dc.titleMSPD procedure combined with GC-MS for the determination of procymidone, bifenthrin, malathion and pirimicarb in honeypt_BR
dc.typeArtigopt_BR
dc.identifier.licenseCreative Commons Atribuição-NãoComercial 4.0 Internacional (CC BY-NC 4.0)pt_BR
dc.description.resumoA method based on matrix solid-phase dispersion and gas chromatography-mass spectrometry to determine procymidone, malathion, bifenthrin and pirimicarb in honey is described. The best results were obtained using 1.0 g of honey, 1.0 g of silica-gel as dispersant sorbent and acetonitrile as eluting solvent. The method was validated by fortified honey samples at three concentration levels (0.2, 0.5 to 1.0 mg kg1 ). Average recoveries (n=7) ranged from 54 to 84%, with relative standard deviations between 3.7 and 8.5%. Detection and quantification limits attained by the developed method ranged from 0.02 to 0.08 mg kg-1 and 0.07 to 0.25 mg kg-1 for the honey, respectively.pt_BR
dc.description.localSão Paulo, SPpt_BR
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